The Role of Calcination Temperature in the Self-cleaning Functionality of Urea-Doped TiO2 Prepared through In Situ Heat-Assisted Sol–Gel Synthesis

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Main Authors: Lukong, Valantine Takwa, Chukwuati, Christopher Nonso, Ukoba, Kingsley
Format: Book
Language:English
Published: Springer 2023
Subjects:
Online Access:https://link.springer.com/article/10.1007/s11665-023-08727-2
https://dlib.phenikaa-uni.edu.vn/handle/PNK/9496
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spelling oai:localhost:PNK-94962023-10-06T08:26:39Z The Role of Calcination Temperature in the Self-cleaning Functionality of Urea-Doped TiO2 Prepared through In Situ Heat-Assisted Sol–Gel Synthesis Lukong, Valantine Takwa Chukwuati, Christopher Nonso Ukoba, Kingsley urea-TiO2 UV irradiation CC-BY In this study, urea-doped titanium dioxide (urea-TiO2) nanoparticles were synthesized through an in situ heat-assisted sol–gel technique using titanium (IV) isopropoxide as the precursor for titanium dioxide and urea as a nitrogen source. The nanoparticles were calcined at 300, 500, and 700 °C to study the effect of the calcination temperature on their function as self-cleaning material. The nanoparticles were characterized using a scanning electron microscope and a transmission electron microscope for morphology, X-ray diffraction, Raman spectroscopy, and Fourier transformed infrared spectroscopy for structure, UV–Vis, and photoluminescence spectroscopy for optical analysis. The self-cleaning study was carried out by letting samples degrade methylene blue and Rhodamine-B under UV irradiation. The morphological analysis reveals particle size distribution with more disparity at higher calcination temperatures. 2023-10-06T08:26:39Z 2023-10-06T08:26:39Z 2023 Book https://link.springer.com/article/10.1007/s11665-023-08727-2 https://dlib.phenikaa-uni.edu.vn/handle/PNK/9496 en application/pdf Springer
institution Digital Phenikaa
collection Digital Phenikaa
language English
topic urea-TiO2
UV irradiation
spellingShingle urea-TiO2
UV irradiation
Lukong, Valantine Takwa
Chukwuati, Christopher Nonso
Ukoba, Kingsley
The Role of Calcination Temperature in the Self-cleaning Functionality of Urea-Doped TiO2 Prepared through In Situ Heat-Assisted Sol–Gel Synthesis
description CC-BY
format Book
author Lukong, Valantine Takwa
Chukwuati, Christopher Nonso
Ukoba, Kingsley
author_facet Lukong, Valantine Takwa
Chukwuati, Christopher Nonso
Ukoba, Kingsley
author_sort Lukong, Valantine Takwa
title The Role of Calcination Temperature in the Self-cleaning Functionality of Urea-Doped TiO2 Prepared through In Situ Heat-Assisted Sol–Gel Synthesis
title_short The Role of Calcination Temperature in the Self-cleaning Functionality of Urea-Doped TiO2 Prepared through In Situ Heat-Assisted Sol–Gel Synthesis
title_full The Role of Calcination Temperature in the Self-cleaning Functionality of Urea-Doped TiO2 Prepared through In Situ Heat-Assisted Sol–Gel Synthesis
title_fullStr The Role of Calcination Temperature in the Self-cleaning Functionality of Urea-Doped TiO2 Prepared through In Situ Heat-Assisted Sol–Gel Synthesis
title_full_unstemmed The Role of Calcination Temperature in the Self-cleaning Functionality of Urea-Doped TiO2 Prepared through In Situ Heat-Assisted Sol–Gel Synthesis
title_sort role of calcination temperature in the self-cleaning functionality of urea-doped tio2 prepared through in situ heat-assisted sol–gel synthesis
publisher Springer
publishDate 2023
url https://link.springer.com/article/10.1007/s11665-023-08727-2
https://dlib.phenikaa-uni.edu.vn/handle/PNK/9496
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