A Limit to Accelerated Free-Sintering: Nano-Phase Separation Interferes With Organic Debinding
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Springer
2023
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Truy cập trực tuyến: | https://link.springer.com/article/10.1007/s11661-023-07152-3 https://dlib.phenikaa-uni.edu.vn/handle/PNK/8960 |
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oai:localhost:PNK-89602023-08-25T08:29:53Z A Limit to Accelerated Free-Sintering: Nano-Phase Separation Interferes With Organic Debinding Naunheim, Yannick Perrin, Alice Olive, Christian E. Nano-Phase Separation Interferes CC-BY Nano-phase separating Ni–12 at. pct Ag powders are processed via high-energy ball milling and brought into a supersaturated state with a reduction of the grain size to the nanocrystalline scale, a combination that is designed to encourage rapid densification by phase separation upon heating. This unstable powder is then characterized by dilatometry, in-situ x-ray diffraction, thermogravimetry and microstructure analysis for sintering cycles up to 940 °C. However, these powder compacts exhibit excessive pore evolution and significant macroscopic swelling caused by removal of the organic process additives. This competition of organic removal with densification is known in nanocrystalline metals, but the present study adds an additional dimension of phase separation, which shifts the dominant swelling mechanism as the formation of the second phase traps the volatilizing organics and hinders the debinding process. 2023-08-25T08:29:53Z 2023-08-25T08:29:53Z 2023 Book https://link.springer.com/article/10.1007/s11661-023-07152-3 https://dlib.phenikaa-uni.edu.vn/handle/PNK/8960 en application/pdf Springer |
institution |
Digital Phenikaa |
collection |
Digital Phenikaa |
language |
English |
topic |
Nano-Phase Separation Interferes |
spellingShingle |
Nano-Phase Separation Interferes Naunheim, Yannick Perrin, Alice Olive, Christian E. A Limit to Accelerated Free-Sintering: Nano-Phase Separation Interferes With Organic Debinding |
description |
CC-BY |
format |
Book |
author |
Naunheim, Yannick Perrin, Alice Olive, Christian E. |
author_facet |
Naunheim, Yannick Perrin, Alice Olive, Christian E. |
author_sort |
Naunheim, Yannick |
title |
A Limit to Accelerated Free-Sintering: Nano-Phase Separation Interferes With Organic Debinding |
title_short |
A Limit to Accelerated Free-Sintering: Nano-Phase Separation Interferes With Organic Debinding |
title_full |
A Limit to Accelerated Free-Sintering: Nano-Phase Separation Interferes With Organic Debinding |
title_fullStr |
A Limit to Accelerated Free-Sintering: Nano-Phase Separation Interferes With Organic Debinding |
title_full_unstemmed |
A Limit to Accelerated Free-Sintering: Nano-Phase Separation Interferes With Organic Debinding |
title_sort |
limit to accelerated free-sintering: nano-phase separation interferes with organic debinding |
publisher |
Springer |
publishDate |
2023 |
url |
https://link.springer.com/article/10.1007/s11661-023-07152-3 https://dlib.phenikaa-uni.edu.vn/handle/PNK/8960 |
_version_ |
1775230275768287232 |
score |
8.891787 |